1: 34.7 g / pyridine / 5 h / Ambient temperature 2: 89 percent / acetonitrile / 1.5 h / Ambient temperature 3: 93 percent / ethanol / 2 h / Ambient temperature View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
1: 2.) 4-chlorophenyl dichlorophosphate / 1.) pyridine, 0 deg C, 12 h, 2.) pyridine, room temperature, 24 h 2: LiN3 / dimethylformamide / 3 h / 50 °C 3: 72 percent / 1N HCl / methanol / 26 h / Ambient temperature 4: 21 percent / H2 / PdCl2 / methanol / 30 h / 2585.7 Torr / Ambient temperature View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
1: 34.7 g / pyridine / 5 h / Ambient temperature
2: 89 percent / acetonitrile / 1.5 h / Ambient temperature
3: aq.ammonia / dioxane / 6 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
1: 34.7 g / pyridine / 5 h / Ambient temperature
2: 89 percent / acetonitrile / 1.5 h / Ambient temperature
3: dioxane; ethanol / 1.5 h / Ambient temperature
4: methanolic ammonia / 16 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
1: 34.7 g / pyridine / 5 h / Ambient temperature
2: 89 percent / acetonitrile / 1.5 h / Ambient temperature
3: dioxane / 2 h / Ambient temperature
4: methanolic ammonia / 16 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
1: 34.7 g / pyridine / 5 h / Ambient temperature
2: 89 percent / acetonitrile / 1.5 h / Ambient temperature
3: pyridine / 4.5 h / Heating
4: methanolic ammionia / 16 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
1: 34.7 g / pyridine / 5 h / Ambient temperature
2: 87 percent / diphenyl phosphorochloridate / pyridine / 3 h / Ambient temperature
3: triethylamine / acetonitrile / 1 h / Ambient temperature
4: methanolic sodium methoxide / 0.25 h / Ambient temperature
View Scheme
参考文献
Divakar, K.J.; Reese, Colin B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1171 - 1176
