2,3,4-三-O-乙酰基-alpha-D-葡萄糖醛酸甲酯合成路线 （共 17 条）
反应条件
benzylamine in N,N-dimethyl-formamide T=20°C; 16 h; Inert atmosphere;
参考文献
Chen, Yi; Li, Yanhong; Yu, Hai; Sugiarto, Go; Thon, Vireak; Hwang, Joel; Ding, Li; Hie, Liana; Chen, Xi
Angewandte Chemie - International Edition, 2013 , vol. 52, # 45 p. 11852 - 11856
Angew. Chem., 2013 , vol. 52, # 45 p. 11852 - 11856,5
反应条件
neodymium trifluoromethanesulfonate in methanol T=20°C; 4 h;
参考文献
Tran, Anh Tuan; Deydier, Sophie; Bonnaffe, David; Le Narvor, Christine
Tetrahedron Letters, 2008 , vol. 49, # 13 p. 2163 - 2165
反应条件
anhydrous cadmium carbonate in water; acetonitrile T=70°C; 4 h;
参考文献
Casati, Silvana; Ottria, Roberta; Ciuffreda, Pierangela
Steroids, 2009 , vol. 74, # 2 p. 250 - 255
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 16 h;
参考文献
Pearson, Andrew G.; Kiefel, Milton J.; Ferro, Vito; Von Itzstein, Mark
Carbohydrate Research, 2005 , vol. 340, # 13 p. 2077 - 2085
反应条件
(tetrabutylammonium)5K[α1-Zr-(H2O)4P2W17O61] T=65°C; 0.166667 h; Microwave irradiationInert atmosphere; chemoselective reaction;
参考文献
Bosco, Michael; Rat, Stephanie; Dupre, Nathalie; Hasenknopf, Bernold; Lacote, Emmanuel; Malacria, Max; Remy, Pauline; Kovensky, Jose; Thorimbert, Serge; Wadouachi, Anne
ChemSusChem, 2010 , vol. 3, # 11 p. 1249 - 1252
反应条件
water; silver carbonate in acetone T=22°C; 24 h; Yield given;
参考文献
Compernolle, Frans
Carbohydrate Research, 1980 , vol. 86, p. 177 - 184
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-60 - 23°C; 41 h; Title compound not separated from byproducts;
参考文献
Engstrom, Kenneth M.; Daanen, Jerome F.; Wagaw, Seble; Stewart, Andrew Q.
Journal of Organic Chemistry, 2006 , vol. 71, # 22 p. 8378 - 8383
反应条件
water; acetic acid 0.25 h; Ambient temperature;
参考文献
Saito; Sumita; Ichinose; Kanda
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 1 p. 90 - 96
反应条件
tri-n-butyltin methoxide in methanol T=50°C; 2 h; other catalyst (Bu2SnO); Product distributionRate constant;
参考文献
Herzig, Jacob; Nudelman, Abraham; Gottlieb, Hugo E.
Carbohydrate Research, 1988 , vol. 177, p. 21 - 28
反应条件
1: pyridine / 24 h / Ambient temperature 2: 30percent aq. HBr / 5 h / Ambient temperature View Scheme
参考文献
Kondo, Hirosato; Aoki, Shin; Ichikawa, Yoshitaka; Halcomb, Randall L.; Ritzen, Helena; Wong, Chi-Huey
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 864 - 877
