(S)-(-)-1-(2-萘基)乙胺合成路线 （共 21 条）
反应条件
anhydrous ammonium carbonate; hydrogenchloride; formic acid 1.) H2O, 183 deg C, 8 h, then 50 deg C, 2 h; 2.) H2O, 110 deg C, 1 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Journal of Molecular Structure, , vol. 475, # 2-3 p. 121 - 130
反应条件
1: With (S)-isopropylidene glycerol 3-carboxy-2-naphthoate in methanol 5 h; Heating; 2: With sulfuric acid in ethyl acetate
参考文献
Tetrahedron Asymmetry, , vol. 13, # 20 p. 2277 - 2282
反应条件
heptakis-(6-O-TIPS)-β-CD; triethylamine in cyclohexane T=10°C; 12 h; Resolution of racemate;
参考文献
Tetrahedron, , vol. 70, # 2 p. 197 - 203
反应条件
trichloroisocyanuric acid; sulfuric acid in water; acetonitrile T=90°C; 18 h;
参考文献
Journal of the American Chemical Society, , vol. 131, p. 8358 - 8359
反应条件
Ni T=110°C; 2 h; Inert atmosphere;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
sodium tetrahydroborate; (S)-valinol; zirconium tetrachloride in tetrahydrofuran Ambient temperature; Title compound not separated from byproducts;
参考文献
Itsuno, Shinichi; Sakurai, Yoshiki; Shimizu, Koji; Ito, Koichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 1859 - 1863
反应条件
1: conc.HCl / tetrahydrofuran 2: 1.) H2, 2.) samarium(II) iodide / 1.) <(COD)Rh(1,2-bis((2R,5R)-2,5-diethylphospholano)-benzene)>+CF3SO3- / 1.) 0 deg C, 12 h, isopropanol, 60 psi; 2.) methanol, THF, 30 min View Scheme
参考文献
Tetrahedron, , vol. 50, # 15 p. 4399 - 4428
反应条件
borane in tetrahydrofuran T=20°C; Yield given;
参考文献
Tetrahedron Letters, , vol. 29, # 2 p. 223 - 224
反应条件
2,6-dimethylpyridine; chiral 1-azaspiro[5.5]undecane N-oxyl radical; sodium perchlorate in water; acetonitrile Oxidation; 5 h; Electrolysis;
参考文献
Chemical Communications, , # 19 p. 1983 - 1984
反应条件
lithium aluminium tetrahydride in diethyl ether a) reflux, 2 h, b) 20 deg C, 12 h;
参考文献
Occhiato, Ernesto; Jones, J. Bryan
Tetrahedron, 1996 , vol. 52, # 12 p. 4199 - 4214
