1: 90 percent / hydrogen / PtO2 / methanol / 12 h / 100 °C / 76000 Torr 2: 96 percent / LiAlH4 / diethyl ether / 3 h / Heating 3: pyridine / 1.) 1 h, 0 deg C; 2.) 4.5 h, 20 deg C 4: LiBr / acetone / 20 °C 5: 1.) Mg / 1.) diethyl ether View Scheme

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1: 90 percent / hydrogen / PtO2 / methanol / 12 h / 100 °C / 76000 Torr 2: NaOH aq. / methanol View Scheme

1: 90 percent / hydrogen / PtO2 / methanol / 12 h / 100 °C / 76000 Torr 2: 96 percent / LiAlH4 / diethyl ether / 3 h / Heating View Scheme