1-乙酰氧基-2,3,5-三苯甲酰氧基-β-L-呋喃核糖合成路线 （共 41 条）
反应条件
sulfuric acid; acetic acid T=0°C;
参考文献
Watanabe, Kyoichi; Choi, Woo-Baeg
Patent: US2005/90660 A1, 2005 ;
Location in patent: Page/Page column 35 ;
反应条件
sulfuric acid; acetic anhydride; sodium hydrogencarbonate in pyridine; methanol; hexane; chloroform; acetic acid; ethyl acetate
反应条件
sulfuric acid; acetic acid T=0 - 20°C;
参考文献
Xiao, Chuan; Sun, Chao; Han, Weiwei; Pan, Feng; Dan, Zhu; Li, Yu; Song, Zhi-Guang; Jin, Ying-Hua
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 23 p. 7100 - 7110
反应条件
sulfuric acid in acetic acid T=-35 - -10°C; 0.25 h;
参考文献
Cimpoia, Alex R.; Hunter, Patricia J.; Evans, Colleen A.; Jin, Haolun; Breining, Tibor; Mansour, Tarek S.
Journal of Carbohydrate Chemistry, 1994 , vol. 13, # 8 p. 1115 - 1120
反应条件
1: L-(+)-ribose With hydrogenchloride in methanol T=20°C; 6 h; 2: benzoyl chloride With pyridine in dichloromethane T=20°C; 3: acetic anhydride With sulfuric acid in acetic acid T=20°C;
参考文献
ICN Pharmaceuticals, Inc.
Patent: EP1254911 A1, 2002 ;
Location in patent: Example 13 ;
反应条件
1: pyridine / 8 h / 20 °C 2: 15 g / AcOH; H2SO4 / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 15 p. 4760 - 4766
反应条件
pyridine; sulfuric acid Cooling with ice;
参考文献
EP2105445 A1, ;
Page/Page column 12-13 ;
反应条件
sulfuric acid in acetic acid Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 24 p. 4199 - 4202
反应条件
sulfuric acid Cooling with ice;
参考文献
EP2105445 A1, ;
Page/Page column 13 ;
反应条件
1: HCl / 2 h / 20 °C 2: pyridine / 8 h / 20 °C 3: 15 g / AcOH; H2SO4 / 0 - 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 15 p. 4760 - 4766
