苄氧羰基-甘氨酰-丙氨酸合成路线 (共 26 条)
反应条件
1: Et3N / CHCl3 / 1 h / Ambient temperature 2: 91 percent / 1 M aq. NaOH / acetone / 3 h / 4 °C View Scheme
参考文献
Kemp,D.S. et al.
Tetrahedron, 1974 , vol. 30, p. 3969 - 3980
反应条件
sodium hydroxide in acetone T=4°C; 3 h;
参考文献
Saito; Shimizu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 10 p. 2974 - 2980
反应条件
triethylamine in water; acetonitrile 16 h;
参考文献
Lebedyeva, Iryna O.; Ostrov, David A.; Neubert, John; Steel, Peter J.; Patel, Kunal; Sileno, Sean M.; Goncalves, Kevin; Ibrahim, Mohamed A.; Alamry, Khalid A.; Katritzky, Alan R.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 4 p. 1479 - 1486
反应条件
sodium hydroxide in methanol
参考文献
Goldschmidt,S.; Gupta,K.K.
Chemische Berichte, 1965 , vol. 98, p. 2831 - 2836
反应条件
sodium hydroxide; sodium hydrogencarbonate in 1,4-dioxane; water
参考文献
Wuensch, E.; Wendlberger, G.; Goehring, W.; Huebener, G.; Traving, B.
Monatshefte fuer Chemie, 1993 , vol. 124, # 5 p. 577 - 586
反应条件
sodium hydroxide in water; butan-1-ol Ambient temperature;
参考文献
Litvinenko, L. M.; Kosmynin, V. V.; Kaida, L. N.; Savelova, V. A.; Verbovaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 4 p. 784 - 785
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 4 p. 877 - 878
反应条件
α-chymotrypsin immobilised on Celite; triethylamine in acetonitrile T=30°C; pH=7.8; 0.5 h;
参考文献
Miyazawa, Toshifumi; Ensatsu, Eiichi; Tanaka, Kayoko; Yanagihara, Ryoji; Yamada, Takashi
Chemistry Letters, 1999 , # 10 p. 1013 - 1014
反应条件
sodium hydroxide; acetone
参考文献
Erlanger; Brand
Journal of the American Chemical Society, 1951 , vol. 73, p. 3508
反应条件
trifluoroacetic acid
参考文献
Waki; Meienhofer
Journal of the American Chemical Society, 1977 , vol. 99, # 18 p. 6075 - 6082
反应条件
1: NaNO2; aqueous acetic acid; aqueous HCl / Behandeln einer Loesung des Reaktionsprodukts in Aether mit L-Alanin-aethylester 2: aqueous NaOH; acetone View Scheme
参考文献
Erlanger; Brand
Journal of the American Chemical Society, 1951 , vol. 73, p. 3508