Barton, Derek H. R.; Donnelly, Dervilla M. X.; Finet, Jean-Pierre; Guiry, Patrick J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , p. 1365 - 1376
1: 96 percent / pyridine / CHCl3 / 3 h / Ambient temperature
2: 74 percent / palladium(II) acetate, 1,2-bis(diphenylphosphino)ethane / acetonitrile / 4 h / Heating
View Scheme
参考文献
Donnelly, Dervilla M.; Finet, Jean-Pierre; Rattigan, Bernard A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 15 p. 1729 - 1736
1: 60 percent / pyridine / CHCl3 / 9 h / 40 °C
2: 68 percent / triethylamine / CH2Cl2 / 8 h / 0 °C
3: 60 percent / HCOOH, triethylamine / triphenylphosphine/Pd(OAc)2 / dimethylformamide / 12 h / 65 °C
View Scheme
参考文献
Donnelly, Dervilla M. X.; Finet, Jean-Pierre; Guiry, Patrick J.; Hutchinson, Rhona M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 10 p. 2851 - 2852
Cu2(OAc)2 in dichloromethane
1 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Donnelly, Dervilla, M. X.; Finet, Jean-Pierre; Guiry, Patrick J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 9 p. 2095 - 2102
1: 84 percent / pyridine / CHCl3 / 10 h / Ambient temperature
2: 91 percent / PPh3, palladium(II) acetate, Et3N, CH2O / tetrahydrofuran / 72 h
View Scheme
参考文献
Donnelly, Dervilla M.; Finet, Jean-Pierre; Rattigan, Bernard A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 15 p. 1729 - 1736
Barton, Derek H. R.; Donnelly, Dervilla M. X.; Finet, Jean-Pierre; Guiry, Patrick J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , p. 1365 - 1376