11H-苯并[b]芴-11-酮合成路线 （共 42 条）
反应条件
1: 91 percent / BaMnO4 / CH2Cl2 / 72 h / 23 °C 2: 32 percent / 14 h / 180 °C / solid state, celite View Scheme
参考文献
Atienza; Mateo; de Frutos; Echavarren
Organic letters, 2001 , vol. 3, # 2 p. 153 - 155
反应条件
1: aq. borax / methanol / 20 °C 2: 70 percent / benzene / 150 °C View Scheme
参考文献
Rodriguez, David; Navarro, Armando; Castedo, Luis; Dominguez, Domingo; Saa, Carlos
Organic Letters, 2000 , vol. 2, # 11 p. 1497 - 1500
反应条件
1.1: magnesium / tetrahydrofuran / 2 h / 20 - 85 °C 1.2: 0 - 20 °C / |Inert atmosphere 2.1: pyridinium chlorochromate; triethylamine / dichloromethane / 20 °C 3.1: palladium diacetate; trifluoroacetic acid; potassium carbonate; silver(l) oxide / 24 h / 140 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Li, Hu; Zhu, Ru-Yi; Shi, Wen-Juan; He, Ke-Han; Shi, Zhang-Jie
Organic Letters, 2012 , vol. 14, # 18 p. 4850 - 4853,4
反应条件
1.1: magnesium / tetrahydrofuran / 2 h / 20 - 85 °C 1.2: 0 - 20 °C / |Inert atmosphere 2.1: pyridinium chlorochromate; triethylamine / dichloromethane / 20 °C 3.1: palladium diacetate; trifluoroacetic acid; potassium carbonate; silver(l) oxide / 24 h / 140 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Li, Hu; Zhu, Ru-Yi; Shi, Wen-Juan; He, Ke-Han; Shi, Zhang-Jie
Organic Letters, 2012 , vol. 14, # 18 p. 4850 - 4853,4
反应条件
1: pyridinium chlorochromate; triethylamine / dichloromethane / 20 °C 2: palladium diacetate; trifluoroacetic acid; potassium carbonate; silver(l) oxide / 24 h / 140 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Li, Hu; Zhu, Ru-Yi; Shi, Wen-Juan; He, Ke-Han; Shi, Zhang-Jie
Organic Letters, 2012 , vol. 14, # 18 p. 4850 - 4853,4
反应条件
1.1: {RuCl2(1-methyl-4-(1-methylethyl)benzene)}2; silver hexafluoroantimonate; silver(l) oxide / tetrahydrofuran / 16 h / 110 °C / |Inert atmosphere 2.1: trifluoroacetic anhydride / 2 h / 100 °C 2.2: 2 h / 100 °C View Scheme
参考文献
Chinnagolla, Ravi Kiran; Jeganmohan, Masilamani
Organic Letters, 2012 , vol. 14, # 20 p. 5246 - 5249,4
反应条件
hydrogenchloride Diazotization;
参考文献
Lothrop; Goodwin
Journal of the American Chemical Society, 1943 , vol. 65, p. 363,365
反应条件
1: concentrated H2SO4 2: copper oxide-chromium oxide; quinoline View Scheme
参考文献
Collins et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 397,399
反应条件
2: aqueous HCl / Diazotization View Scheme
参考文献
Lothrop; Goodwin
Journal of the American Chemical Society, 1943 , vol. 65, p. 363,365
反应条件
1: 80 percent / n-BuLi / tetrahydrofuran; hexane / 5 h / 0 - 23 °C 2: 91 percent / BaMnO4 / CH2Cl2 / 72 h / 23 °C 3: 32 percent / 14 h / 180 °C / solid state, celite View Scheme
参考文献
Gonzalez-Cantalapiedra, Esther; De Frutos, Oscar; Atienza, Carmen; Mateo, Cristina; Echavarren, Antonio M.
European Journal of Organic Chemistry, 2006 , # 6 p. 1430 - 1443
