11H-苯并[b]芴-11-酮合成路线 （共 42 条）
反应条件
pyridine-2-carboxylic acid; sodium tetrahydroborate; bismuth(III)oxide; tert.-butylhydroperoxide in pyridine; water; acetic acid T=100°C; 16 h;
参考文献
Bonvin, Yannick; Callens, Emmanuel; Larrosa, Igor; Henderson, David A.; Oldham, James; Burton, Andrew J.; Barrett, Anthony G. M.
Organic Letters, 2005 , vol. 7, # 21 p. 4549 - 4552
反应条件
γ-terpinene in toluene T=180°C; 79 h;
参考文献
Gonzalez-Cantalapiedra, Esther; De Frutos, Oscar; Atienza, Carmen; Mateo, Cristina; Echavarren, Antonio M.
European Journal of Organic Chemistry, 2006 , # 6 p. 1430 - 1443
反应条件
sodium ethanolate in ethanol 1.) overnight, 2.) reflux, 24 h;
参考文献
Streitweiser, Andrew; Brown, Sandra M.
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 904 - 906
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Rodriguez, David; Martinez-Esperon, Maria Fernanda; Navarro-Vazquez, Armando; Castedo, Luis; Dominguez, Domingo; Saa, Carlos
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3842 - 3848
反应条件
in toluene T=150°C; Cyclization; 13 h;
参考文献
Rodriguez, David; Navarro, Armando; Castedo, Luis; Dominguez, Domingo; Saa, Carlos
Organic Letters, 2000 , vol. 2, # 11 p. 1497 - 1500
反应条件
palladium diacetate; silver(l) oxide in trifluoroacetic acid T=130°C; 36 h; Inert atmosphere;
参考文献
Gandeepan, Parthasarathy; Hung, Chen-Hsun; Cheng, Chien-Hong
Chemical Communications, 2012 , vol. 48, # 75 p. 9379 - 9381
反应条件
polyphosphoric acid T=120°C; Friedel Crafts reaction; 12 h; regioselective reaction;
参考文献
Kim, Ko Hoon; Kim, Sung Hwan; Lee, Ka Young; Kim, Jae Nyoung
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 4 p. 1387 - 1390
反应条件
1: With trifluoroacetic anhydride T=100°C; 2 h; 2: With hydrogenchloride in water T=100°C; 2 h;
参考文献
Chinnagolla, Ravi Kiran; Jeganmohan, Masilamani
Organic Letters, 2012 , vol. 14, # 20 p. 5246 - 5249,4
反应条件
1: MnO2 / CH2Cl2 / 20 °C 2: 61 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C View Scheme
参考文献
Rodriguez, David; Navarro, Armando; Castedo, Luis; Dominguez, Domingo; Saa, Carlos
Organic Letters, 2000 , vol. 2, # 11 p. 1497 - 1500
反应条件
sulfuric acid in 1,2-dichloro-ethane 4 h; Reflux;
参考文献
Kim, Ko Hoon; Kim, Sung Hwan; Lee, Ka Young; Kim, Jae Nyoung
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 4 p. 1387 - 1390
