1-甲氧基-3-苯磺酰基苯合成路线 （共 23 条）
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; copper(II) bis(trifluoromethanesulfonate); caesium carbonate in N,N-dimethyl-formamide T=110°C; Ullmann reaction; 6 h; Inert atmosphere;
参考文献
Prasad; Sekar, Govindasamy
Synthesis, 2010 , # 1 p. 79 - 84
反应条件
copper(I) oxide; caesium carbonate; ethyl 2-oxo-cyclohexanecarboxylate in dimethyl sulfoxide T=80°C; 20 h;
参考文献
Xu, Hua-Jian; Zhao, Xiao-Yang; Deng, Jin; Fu, Yao; Feng, Yi-Si
Tetrahedron Letters, 2009 , vol. 50, # 4 p. 434 - 437
反应条件
1: iodobenzene With (R)-(+)-1,1'-binaphthyl-2,2'-diamine; copper diacetate; potassium ethylxanthate in N,N-dimethyl-formamide T=105°C; Ullmann type reaction; 20 h; Inert atmosphere; 2: 3-methoxy-iodobenzene With potassium hydroxide in N,N-dimethyl-formamide T=105°C; 24 h; Inert atmosphere;
参考文献
Prasad; Sekar, Govindasamy
Organic Letters, 2011 , vol. 13, # 5 p. 1008 - 1011
反应条件
1: bromobenzene With 1,2,3-Benzotriazole; copper(l) iodide in dimethyl sulfoxide 0.166667 h; 2: 3-methoxy-benzenethiol With potassium tert-butylate in dimethyl sulfoxide T=100°C; Further stages.;
参考文献
Verma, Akhilesh Kumar; Singh, Jaspal; Chaudhary, Ritu
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7199 - 7202
反应条件
potassium carbonate in N,N-dimethyl-formamide T=120°C; 0.0833333 h; microwave irradiation;
参考文献
Ranu, Brindaban C.; Saha, Amit; Jana, Ranjan
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2690 - 2696
反应条件
potassium tert-butylate in dimethyl sulfoxide T=40 - 80°C; Overall yield = 81 percent; Overall yield = 0.17 g;
参考文献
Kumar, Sangit; Kumar, Amit; Bhakuni, Bhagat Singh; Prasad, Ch. Durga; Kumar, Shailesh
Tetrahedron, 2013 , vol. 69, # 26 p. 5383 - 5392
反应条件
cesium fluoride in acetonitrile T=20°C; 24 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; bis(dibenzylideneacetone)-palladium(0); thiolacetic acid potassium salt in acetone; toluene T=70 - 110°C; 9 h; Inert atmosphere;
参考文献
Park, Namjin; Park, Kyungho; Jang, Mihee; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4371 - 4378
反应条件
tetrakis(triphenylphosphine) palladium(0); (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl; potassium hydroxide in isopropyl alcohol T=83°C; Migita-Sano Synthesis; 21 h; Inert atmosphere;
参考文献
Norris, Timothy; Leeman, Kyle
Organic Process Research and Development, 2008 , vol. 12, # 5 p. 869 - 876
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; bis(dibenzylideneacetone)-palladium(0); thiolacetic acid potassium salt in acetone; toluene T=70 - 110°C; 9 h; Inert atmosphere;
参考文献
Park, Namjin; Park, Kyungho; Jang, Mihee; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4371 - 4378
