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Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 10 p. 1559 - 1570
1: 2-ethylacetoacetic acid ethyl ester With lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 0.5 h; 2: formaldehyd in tetrahydrofuran T=-78 - 20°C; Further stages.;
参考文献
Beddow, James E.; Davies, Stephen G.; Ling, Kenneth B.; Roberts, Paul M.; Russell, Angela J.; Smith, Andrew D.; Thomson, James E.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 17 p. 2812 - 2825
dimethylcopper lithium in diethyl ether T=-80°C; other unsaturated esters, other metaloorganic compounds, various temperatures and solvents; Product distribution;
参考文献
Amri, Hassen; Rambaud, Monique; Villieras, Jean
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 1 - 11