反式-环戊烷-1,2-二羧酸二乙酯合成路线 (共 2 条)
反应条件
1: LiAlH4 2: PBr3 3: aq. ethanol / Heating 4: H2SO4 5: (i) LiAlH4, (ii) PBr3, (iii) /BRN= 4652394/ 6: (i) LiNMePh, (ii) aq. HCl, (iii) aq. H2SO4 7: aq. N2H4, KOH / bis-(2-hydroxy-ethyl) ether View Scheme
参考文献
Allinger,N.L.; Zalkow,V.B.
Journal of the American Chemical Society, 1961 , vol. 83, p. 1144 - 1146
反应条件
With ethanol; toluene-4-sulfonic acid
参考文献
Owen; Peto Journal of the Chemical Society, 1955 , p. 2383,2386 Blomquist et al. Journal of the American Chemical Society, 1956 , vol. 78, p. 6057,6063