2-乙酰氨基-3,4,6-三-O-乙酰-2-脱氧-α-D-吡喃葡萄糖酰基氯合成路线 （共 104 条）
反应条件
1: 71 percent / silver trifluoromethanesulfonate / CH2Cl2 / 2 h / 0 °C 2: 81 percent / NaOMe / methanol / 3 h / 20 °C View Scheme
参考文献
Zemlyakov; Kur'yanov; Tsikalov; Aksenova; Chirva
Chemistry of Natural Compounds, 1997 , vol. 33, # 1 p. 61 - 66
反应条件
3 A molecular sieve; mercury(II) iodide in dichloromethane
参考文献
Chemistry of Natural Compounds, , vol. 33, # 1 p. 61 - 66
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: cobalt(II) chloride / dichloromethane / 3 h / 50 °C View Scheme
参考文献
Kuryanov; Luschtshyk; Chupakhina
Russian Journal of Bioorganic Chemistry, 2013 , vol. 39, # 4 p. 426 - 433
Biokhimiya (Moscow), 2013 , vol. 39, # 4 p. 477 - 485
反应条件
1: sodium azide / acetone / 16 h / |Reflux 2: sodium methylate; methanol / 2 h / 0 °C 3: human His6-propeptide-placental catβ1,4-galactosyltransferase 1 fusion protein; Campylobacter jejuni UDP-Glc/GlcNAc-4'-epimerase; alkaline phosphatase / |Enzymatic reaction View Scheme
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
反应条件
isopropenylbenzene T=160°C; 0.3 h; Yield given;
参考文献
Nishizawa, Mugio; Shimomoto, Waka; Momii, Fumiko; Yamada, Hidetoshi
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1907 - 1908
反应条件
1: 74 percent / tetrabutylammonium hydrogen sulfate, NaOH / CH2Cl2; H2O / 1.4 h 2: 94 percent / NaOMe, MeOH / 5 °C View Scheme
参考文献
Roy, Rene; Tropper, Francois D.; Morrison, Tara; Boratynski, Janusz
Journal of the Chemical Society, Chemical Communications, 1991 , # 7 p. 536 - 538
反应条件
1: in N,N-dimethyl-formamide T=20°C; 16 h; 2: With sodium methylate in methanol
参考文献
Carmona, Ana T.; Fialova, Pavla; Kren, Vladimir; Ettrich, Rudiger; Martinkova, Ludmila; Moreno-Vargas, Antonio J.; Gonzalez, Cristina; Robina, Inmaculada
European Journal of Organic Chemistry, 2006 , # 8 p. 1876 - 1885
反应条件
mercury(II) cyanide in benzene
参考文献
Kauth; Kunz
1983 , vol. No. 3, p. 360 - 366
反应条件
1: 94 percent / mercuric cyanide / 24 h / 20 °C 2: 85 percent / methanol; sodium methoxide / 3 h / 20 °C View Scheme
参考文献
Leaback; Walker
Journal of the Chemical Society, 1957 , p. 4754,4757
反应条件
1.1: acetonitrile / 0.17 h / 20 °C / Molecular sieve 1.2: 25 h / 55 - 80 °C 2.1: sodium methylate / methanol / 2 h / 20 °C 2.2: Amberlite IR-120 (H+ form) 3.1: Jack bean N-acetyl-β-D-glucosaminidase / isopropyl alcohol / 48 h / 37 °C / pH 5 / aq. sodium phosphate buffer; Enzymatic reaction View Scheme
参考文献
Garcia-Alvarez, Isabel; Groult, Hugo; Casas, Josefina; Barreda-Manso, M. Asuncion; Yanguas-Casas, Natalia; Nieto-Sampedro, Manuel; Romero-Ramirez, Lorenzo; Fernandez-Mayoralas, Alfonso
Journal of Medicinal Chemistry, 2011 , vol. 54, # 19 p. 6949 - 6955
