2-乙酰氨基-3,4,6-三-O-乙酰-2-脱氧-α-D-吡喃葡萄糖酰基氯合成路线 （共 104 条）
反应条件
1: molecular sieves 4 Angstroem; Hg(CN)2 / nitromethane; toluene / 20 °C 2: NaOMe / methanol / 0.5 h / 20 °C View Scheme
参考文献
Vega-Perez, Jose M.; Palo-Nieto, Carlos; Perinan, Ignacio; Vega-Holm, Margarita; Calderon-Montano, Jose M.; Lopez-Lazaro, Miguel; Iglesias-Guerra, Fernando
European Journal of Organic Chemistry, 2012 , # 6 p. 1237 - 1252
反应条件
1: dichloromethane / 16 h / 20 °C 2: sodium methylate; methanol / 2 h / 0 °C View Scheme
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
反应条件
15-crown-5; sodium iodide in 1,2-dichloro-ethane T=70°C; Title compound not separated from byproducts;
参考文献
Kur'yanov; Zemlyakov; Chupakhina; Chirva
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 4 p. 282 - 283
反应条件
15-crown-5; sodium iodide in 1,2-dichloro-ethane Ambient temperature;
参考文献
Kur'yanov; Zemlyakov; Chupakhina; Chirva
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 4 p. 282 - 283
反应条件
15-crown-5; sodium iodide Ambient temperatureother alcohols, var. temp.;
参考文献
Kur'yanov; Zemlyakov; Chupakhina; Chirva
Russian Journal of Bioorganic Chemistry, 1998 , vol. 24, # 4 p. 282 - 283
反应条件
1: 80 percent / 4 Angstroem mol sieves, Hg(CN)2 / nitromethane; toluene / Ambient temperature 2: NaOMe / methanol / 30 h / Ambient temperature View Scheme
参考文献
Iglesias-Guerra, Fernando; Romero, Isidora; Alcudia, Felipe; Vega-Perez, Jose M.
Carbohydrate Research, 1998 , vol. 308, # 1-2 p. 57 - 62
反应条件
1: NaN3; nBu4NHSO4; aq. NaHCO3 / CH2Cl2 / 2 h / 20 °C 2: H2; Et3N / Pd/C / ethyl acetate / 0.5 h View Scheme
参考文献
Organic Letters, , vol. 8, # 22 p. 5009 - 5012
反应条件
in acetone T=60°C; 2 h; Product distribution / selectivity;
参考文献
ISIS INNOVATION LIMITED
Patent: WO2005/862 A2, 2005 ;
Location in patent: Page/Page column 22 ;
反应条件
4 A molecular sieve; tetra(n-butyl)ammonium hydrogensulfate in acetonitrile 1.) room temp., 3 h, 2.) reflux, 3 h;
参考文献
Camarasa, M. Jose; Fernandez-Resa, Piedad; Garcia-Lopez, M. Teresa; Heras, Federico G. de las; Mendez-Castrillon, Paloma P.; Felix, Ana San
Synthesis, 1984 , # 6 p. 509 - 510
反应条件
silver trifluoromethanesulfonate in dichloromethane T=0°C; 2 h;
参考文献
Sarkar, Arun K; Brown, Jillian R; Esko, Jeffrey D
Carbohydrate Research, 2000 , vol. 329, # 2 p. 287 - 300
