2,3,4-三-O-乙酰基-α-D-木吡喃糖苷溴合成路线 (共 37 条)
反应条件
hydrogen bromide in dichloromethane; acetic acid T=0 - 20°C; 3 h;
参考文献
Mitchell; Pratt; Hruby; Polt
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2327 - 2342
反应条件
trimethylsilyl bromide in dichloromethane T=-40 - 20°C; 72 h; other solvent;
参考文献
Spencer, Roxanne P.; Cavallaro, Cullen L.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3987 - 3995
反应条件
1: 100 percent / pyridine / 24 h / 0 °C 2: 91 percent / HBr; AcOH / 20 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 20 p. 3897 - 3900
反应条件
trimethylsilyl bromide in dichloromethane
参考文献
Journal of Organic Chemistry, , vol. 60, # 21 p. 7055 - 7057
反应条件
phosphorus; perchloric acid; bromine
参考文献
Sun, Xiaofei; Ji, Li; Ren, Sumei; Wan, Shengbiao; Jiang, Tao
Synthetic Communications, 2008 , vol. 38, # 23 p. 4116 - 4124
参考文献
Journal of the American Chemical Society, , vol. 76, p. 3224
反应条件
1: pyridine 2: hydrogen bromide View Scheme
参考文献
Carbohydrate Research, , vol. 349, p. 12 - 23
反应条件
perchloric acid Eintragen von Phosphor und Brom in das Reaktionsgemisch;
参考文献
Chemische Berichte, , vol. 87, p. 1488,1490
反应条件
1: silver chloride; diethyl ether 2: silver chloride; diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 63, p. 2292,2297
反应条件
[Cp2Ti(III)Cl]2 in tetrahydrofuran Ambient temperature;
参考文献
Spencer, Roxanne P.; Cavallaro, Cullen L.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3987 - 3995