2,3-二甲氧基-5-甲基-1,4-苯二酚合成路线 （共 43 条）
反应条件
sodium dithionite in 1,2-dichloro-ethane T=20°C; 3 h;
参考文献
Yu, Xiong-Jie; Chen, Fen-Er; Dai, Hui-Fang; Chen, Xu-Xiang; Kuang, Yun-Yan; Xie, Bin
Helvetica Chimica Acta, 2005 , vol. 88, # 10 p. 2575 - 2581
反应条件
in xylene 1.25 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 112, # 5 p. 1897 - 1905
反应条件
1: 47 percent / 30percent H2O2, HOAc / 192 h / Ambient temperature 2: 92.1 percent / NaBH4 / H2O; diethyl ether; methanol / 0.25 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 14 p. 3303 - 3310
反应条件
1: Al(OiPr)3 / propan-2-ol 2: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3 3: K2CO3 / acetone 4: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
反应条件
1: NO2/HNO3 / acetic acid 2: Al(OiPr)3 / propan-2-ol 3: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3 4: K2CO3 / acetone 5: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
反应条件
1: K2CO3, KI / acetone 2: aq. H2SO4 / acetic acid 3: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3 4: K2CO3 / acetone 5: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
反应条件
1: (i) H2, aq. HCl, Pd-C, (ii) FeCl3, aq. HCl 2: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
反应条件
1: Al(OiPr)3 / propan-2-ol 2: (i) H2, aq. HCl, Pd-C, (ii) FeCl3, aq. HCl 3: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
反应条件
1: K2CO3 / acetone 2: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
反应条件
1: (i) H2, aq. HCl, Pd-C, (ii) aq. FeCl3 2: K2CO3 / acetone 3: aq. Na2S2O3 / diethyl ether View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 16, p. 2343 - 2350
