H-VAL-GLU-OH合成路线 （共 12 条）
反应条件
1: dicyclohexylcarbodiimide 2: catalytic hydrogenation View Scheme
参考文献
Baba,Y. et al.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 215 - 220
反应条件
hydrogen; palladium(IV) oxide in methanol; acetic acid
参考文献
McGregor,W.H.; Carpenter,F.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1849 - 1854
反应条件
1: (i) PCl5, Et2O, (ii) /BRN= 1726671/ 2: KOH / ethanol 3: H2 / PdO2 / methanol; acetic acid View Scheme
参考文献
McGregor,W.H.; Carpenter,F.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1849 - 1854
反应条件
1: (i) PCl5, Et2O, (ii) /BRN= 1726671/ 2: KOH / ethanol 3: H2 / PdO2 / methanol; acetic acid View Scheme
参考文献
McGregor,W.H.; Carpenter,F.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1849 - 1854
反应条件
1: KOH / ethanol 2: H2 / PdO2 / methanol; acetic acid View Scheme
参考文献
McGregor,W.H.; Carpenter,F.H.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1849 - 1854
反应条件
hydrogen; palladium on activated charcoal in acetic acid
参考文献
Ohyama, Satoshi; Ishibashi, Norio; Tamura, Masahiro; Nishizaki, Hiroshi; Okai, Hideo
Agricultural and Biological Chemistry, 1988 , vol. 52, # 3 p. 871 - 872
反应条件
methanol; palladium Hydrogenation;
参考文献
Martynov, V. F.; Anokhina, V. V.; Belokrylov, G. A.; Leont'eva, L. I.; Sorochinskaya, E. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 10 p. 2369 - 2377,2122 - 2128
反应条件
1: 65 percent / 1 N NaOH 2: hydrogen / Pd-C / methanol / 4 h View Scheme
参考文献
Martynov, V. F.; Anokhina, V. V.; Belokrylov, G. A.; Leont'eva, L. I.; Sorochinskaya, E. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 10 p. 2369 - 2377,2122 - 2128
反应条件
1: 65 percent / 1 N NaOH 2: hydrogen / Pd-C / methanol / 4 h View Scheme
参考文献
Martynov, V. F.; Anokhina, V. V.; Belokrylov, G. A.; Leont'eva, L. I.; Sorochinskaya, E. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 10 p. 2369 - 2377,2122 - 2128
反应条件
1: dicyclohexyl-carbodiimide / dichloromethane / 20 °C / Cooling with ice 2: water; sodium hydroxide / methanol / 10 h 3: trifluoroacetic acid / 8 h View Scheme
参考文献
Naskar, Jishu; Roy, Subhasish; Joardar, Anindita; Das, Sumantra; Banerjee, Arindam
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 19 p. 6610 - 6615
