反应条件
water in hexane byproducts: Me3Si(CCH); stirring (evacuated sealed ampul, -30°C, 5 h), hydrolysis; distn. (vac.), chromy. of residue (column of silica gel, ether/hexane 1:10); elem. anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Vyazankina, O. A.; Medvedeva, A. S.; Safronova, L. P.; Vyazankin, N. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1733 - 1734
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1897 - 1898
