2,2-二氯-1,1,1-三氟乙烷合成路线 （共 115 条）
反应条件
nitrogen trifluoride; hydrogen fluoride; oxygen; chromium based-catalyst
Further byproducts. Title compound not separated from byproducts.;
参考文献
Belter, Randolph K.; Sweval, Mark S.; Iikubo, Yuichi
Journal of Fluorine Chemistry, 2006 , vol. 127, # 6 p. 816 - 820
反应条件
copper
T=60°C; 12 h;
参考文献
Xu, Yuelian; Dolbier Jr., William R.; Rong, Xiao X.
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1576 - 1577
反应条件
diethylamine; copper
T=20°C; P=915.2 - 1018.63 Torr; 64 h; Inert atmosphere; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/117458 A2, 2009 ;
Location in patent: Page/Page column 8-9 ;
反应条件
[2,2']bipyridinyl; copper(I) chloride; copper in N,N-dimethyl-formamide
T=20 - 80°C; P=992.774 - 1303.07 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/117458 A2, 2009 ;
Location in patent: Page/Page column 4-5 ;
反应条件
diethylamine; copper
T=20°C; P=915.2 - 1018.63 Torr; 64 h; Inert atmosphere; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/117458 A2, 2009 ;
Location in patent: Page/Page column 8-9 ;
反应条件
copper(I) chloride; copper
T=20 - 80°C; P=966.916 - 1328.93 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/117458 A2, 2009 ;
Location in patent: Page/Page column 7-8 ;
反应条件
copper; diethylamine; triethylamine
T=75°C; 24 h; Inert atmosphereSealed tube; ConcentrationTemperature;
参考文献
Tang, Xiao-Jun; Chen, Qing-Yun
Organic Letters, 2012 , vol. 14, # 24 p. 6214 - 6217
反应条件
UV-Licht.Irradiation;
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
反应条件
UV-Licht.Irradiation;
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
