2,2-二氯-1,1,1-三氟乙烷合成路线 （共 115 条）
反应条件
zinc; copper(l) chloride 1.) DMF, 24 h; 2.) DMF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tamura, Masanori; Sekiya, Akira
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 119 - 122
反应条件
water; zinc unter Zusatz eines Netzmittels;
参考文献
Kellogg Co.
Patent: US2774798 , 1954 ;
反应条件
zinc; copper(l) chloride in N,N-dimethyl-formamide Ambient temperaturevarious concentrations; without catalyst; further aldehydes; Product distributionMechanism;
参考文献
Journal of Fluorine Chemistry, , vol. 71, # 1 p. 119 - 122
反应条件
diethylamine; copper T=20°C; P=915.2 - 1018.63 Torr; 64 h; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2009/117458 A2, ;
Page/Page column 8-9 ;
反应条件
copper(I) chloride; copper T=20 - 80°C; P=966.916 - 1328.93 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
WO2009/117458 A2, ;
Page/Page column 7-8 ;
反应条件
AlCl3, aluminium chloride T=50 - 52°C; P=4121.6 - 5931.67 Torr; 6 h; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/30442 A1, 2008 ;
Location in patent: Page/Page column 9-10 ;
反应条件
(i) nBuLi, (ii) /BRN= 635680/; Multistep reaction;
参考文献
Seyferth,D. et al.
Organometallics in Chemical Synthesis, 1970 , vol. 1, p. 3 - 6
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
反应条件
hydrogen fluoride; fluorinated chromium oxide
T=320°C; P=2353.83 Torr; 60 h;
参考文献
Daikin Industries, Ltd.
Patent: US6392106 B1, 2002 ;
Location in patent: Page column 5-7 ;
