KNH2 in acetone
T=-38°C; chemical or electrochemical reductive stimulation of the reaction of various nucleophiles, at various catalysts; MechanismRate constant;
参考文献
Amatore, Christian; Oturan, Mehmet A.; Pinson, Jean; Saveant, Jean-Michel; Thiebault, Andre
Journal of the American Chemical Society, 1985 , vol. 107, p. 3451 - 3459
1: With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
24 h; Heating / reflux;
2: With potassium fluoride in 1,4-dioxane; diethyl ether; water
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/54202 A1, 2005 ;
Location in patent: Page/Page column 42 ;
WO 2005/054202 A1