1,3,5-三氨基-2,4,6-三硝基苯合成路线 （共 30 条）
反应条件
ammonia in toluene 10 h; Heating;
参考文献
Kohne, Bernd; Praefcke, Klaus
Liebigs Annalen der Chemie, 1985 , # 3 p. 522 - 528
反应条件
DAHP in sulfolane T=20 - 177°C; 8 h;
参考文献
Mitchell, Alexander R.; Coburn, Michael D.; Lee, Gregory S.; Schmidt, Robert D.; Pagoria, Philip F.; Hsu, Peter C.
Patent: US2005/70743 A1, 2005 ;
Location in patent: Page/Page column 2; sheet 2 ;
反应条件
ammonia in toluene T=90°C; P=3863.02 Torr; 4 h; Product distribution / selectivity;
参考文献
Alliant Techsystems Inc.
Patent: US7763753 B1, 2010 ;
Location in patent: Page/Page column 9-10 ;
反应条件
ammonia in water; N,N-dimethyl-formamide T=20 - 130°C; P=8791.75 Torr; 0.666667 - 2.5 h; Product distribution / selectivity;
参考文献
The Regents of the University of California.
Patent: US2005/38297 A1, 2005 ;
Location in patent: Page/Page column 5; 6 ;
反应条件
4-amino-1,2,4-(4H)triazole; sodium methylate in methanol T=25 - 60°C; 21.5 h; Product distribution / selectivity;
参考文献
The Regents of the University of California.
Patent: US2005/38297 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
ammonia in water T=123°C; 1 h;
参考文献
The Regents of the University of California.
Patent: US2005/38297 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
ammonia in diethyl ether
参考文献
US2005/70743 A1, ;
Page/Page column sheet 2 ;
反应条件
1: With sodium methylate in methanol; dimethyl sulfoxide; toluene T=25 - 90°C; 2.33333 h; 2: With acetic acid in dimethyl sulfoxide; toluene Product distribution / selectivity;
参考文献
The Regents of the University of California.
Patent: US2005/38297 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
ammonia in tetrachloromethane; toluene 0.583333 h;
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
1: 78 percent / 96percent H2SO4, 90percent HNO3 / acetic acid / 9 h / 0 °C 2: 35 percent / 96percent aq. H2SO4 / 60 h / 0 °C 3: 40 percent / 90percent HNO3, 100percent H2SO4 / 1.) RT, 60 min, 2.) 75 deg C, 90 min 4: 97 percent / anh. ammonia / toluene; CCl4 / 0.58 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 17 p. 3261 - 3266
