5,5-二甲基-2-(苯氧基)-1,3,2-二氧磷杂环己烷合成路线 (共 9 条)
反应条件
triethylamine in toluene T=0°C; 0.5 h;
参考文献
Khatib, F. el; Caminade, A. M.; Koenig, M.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 20, p. 55 - 66
反应条件
1: toluene / 8 h / -40 - 20 °C 2: water; potassium carbonate View Scheme
参考文献
Satish Kumar; Kumaraswamy, Sudha; Said, Musa A.; Kumara Swamy
Organic Process Research and Development, 2003 , vol. 7, # 6 p. 925 - 928
反应条件
sodium unter vermindertem Druck;
参考文献
Arshinova, R.P.; Kadyrov, R.A.; Klochkov, V.V.; Aganov, A.V.; Shakirov, I.Kh.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2301 - 2305
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2512 - 2517
反应条件
water; potassium carbonate Reagent/catalyst;
参考文献
Satish Kumar; Kumaraswamy, Sudha; Said, Musa A.; Kumara Swamy
Organic Process Research and Development, 2003 , vol. 7, # 6 p. 925 - 928
反应条件
water in tetrahydrofuran T=25°C; Yield given;
参考文献
Satish Kumar; Kumaraswamy, Sudha; Said, Musa A.; Kumara Swamy
Organic Process Research and Development, 2003 , vol. 7, # 6 p. 925 - 928
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide in chlorobenzene T=30°C; KineticsMechanism;
参考文献
Rueger, C.; Koenig, T.; Schwetlick, K.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 4 p. 622 - 632
反应条件
in 1,2-dichloro-ethane
参考文献
Clovis,J.S.; Sullivan,F.R.
Tetrahedron Letters, 1971 , # 25 p. 2263 - 2266
反应条件
dinitrogen tetraoxide in dichloromethane
T=-60°C;
参考文献
Caminade, A. M.; Khatib, F. El; Koenig, M.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 18, p. 97 - 100
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide in chlorobenzene
T=30°C; KineticsMechanism;
参考文献
Rueger, C.; Koenig, T.; Schwetlick, K.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 4 p. 622 - 632