甲基 2-(乙酰基氨基)-2-脱氧-D-吡喃葡萄糖苷合成路线 (共 9 条)
反应条件
acetyl chloride 23 h;
参考文献
Emmerson, Daniel P G; Villard, Renaud; Mugnaini, Claudia; Batsanov, Andrei; Howard, Judith A K; Hems, William P; Tooze, Robert P; Davis, Benjamin G
Organic and biomolecular chemistry, 2003 , vol. 1, # 21 p. 3826 - 3838
反应条件
methanol; acetyl chloride 1.5 h; Heating;
参考文献
Yoshikawa; Kamigauchi; Ikeda; Kitagawa
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 9 p. 2582 - 2586
反应条件
in methanol Inert atmosphere;
参考文献
Boutureira, Omar; McGouran, Joanna F.; Stafford, Robert L.; Emmerson, Daniel P. G.; Davis, Benjamin G.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 20 p. 4285 - 4288
反应条件
toluene-4-sulfonic acid 24 h; Heating;
参考文献
Kida, Toshiyuki; Yurugi, Keiji; Masuyama, Araki; Nakatsuji, Yohji; Ono, Daisuke; Takeda, Tokuji
Journal of the American Oil Chemists' Society, 1995 , vol. 72, # 7 p. 773 - 780
反应条件
in pyridine 1.) 1 h, 0 deg C, 2.) 16 h, RT;
参考文献
Kovac; Edgard
Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2455 - 2467
反应条件
1: pyridine View Scheme
参考文献
Kovac; Edgard
Journal of Organic Chemistry, 1992 , vol. 57, # 8 p. 2455 - 2467
反应条件
zinc(II) chloride Ambient temperature; Title compound not separated from byproducts;
参考文献
Thiel, Gerhard; Beck, Wolfgang
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 9 p. 1081 - 1093
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=70°C; 2.5 h;
参考文献
Organic and biomolecular chemistry, , vol. 1, # 21 p. 3826 - 3838
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=70°C;
参考文献
Journal of Organic Chemistry, , vol. 76, # 9 p. 3502 - 3505