反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '2039306', constants.ctx, '0')">4-Hydroxybenzenethiol</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '8128150', constants.ctx, '0')">sodium hydroxide</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a>; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />T=-5°C; 1.5 h; Large scale; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '878140', constants.ctx, '0')">2-bromo-1-ethanol</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a>; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />T=-5 - 20°C; 21.25 h; Large scale; <br />
参考文献
Scalone, Michelangelo; Waldmeier, Pius Organic Process Research and Development, 2003 , vol. 7, # 3 p. 418 - 425
