4,5,6-三甲氧基-1H-吲哚合成路线 (共 8 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 20 deg C --> reflux;
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
sodium hydroxide in methanol 7 h; Heating;
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
1: 60 percent / aeration / 2.5 h 2: 13 percent / lithium aluminium hydride View Scheme
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
1: 1.) boron trichloride / 1) 1,2-dichloroethane, ice-cooling; 2) reflux, 3 h 2: sodium borohydride / dioxane; H2O / 1.5 h / Heating View Scheme
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
sodium tetrahydroborate in 1,4-dioxane; water 1.5 h; Heating;
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
1: 6.3 g / pyridine / 108 h / 20 °C 2: 40 percent / hydrochloric acid / dioxane / 1.5 h / Heating 3: 30 percent / aq. sodium hydroxide / methanol / 7 h / Heating View Scheme
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
1: 40 percent / hydrochloric acid / dioxane / 1.5 h / Heating 2: 30 percent / aq. sodium hydroxide / methanol / 7 h / Heating View Scheme
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911
反应条件
lithium aluminium tetrahydride
参考文献
Hewlins, Michael J. E.; Jackson, Anthony H.; Oliveira-Campos Ana-M.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2906 - 2911