3,4,5-三甲氧基苯甲酰乙酸乙酯合成路线 (共 23 条)
反应条件
sodium hydride in toluene; mineral oil
参考文献
Chen, Yi-Fong; Lin, Yi-Chien; Huang, Po-Kai; Chan, Hsu-Chin; Kuo, Sheng-Chu; Lee, Kuo-Hsiung; Huang, Li-Jiau
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 17 p. 5064 - 5075
反应条件
molybdenium(VI) dioxodichloride in dichloromethane T=20°C; 5 h;
参考文献
Jeyakumar, Kandasamy; Chand, Dillip Kumar
Synthesis, 2008 , # 11 p. 1685 - 1687
反应条件
ammonium hydroxide T=20°C;
参考文献
Li, Yao-Wu; Liu, Jia; Liu, Na; Shi, Duo; Zhou, Xiao-Tian; Lv, Jia-Guo; Zhu, Ju; Zheng, Can-Hui; Zhou, You-Jun
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 11 p. 3579 - 3584
反应条件
1: diethyl ether; dioxane 2: NaH; dibutyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2923
反应条件
sodium ethanolate T=0 - 5°C;
参考文献
Zhu, Youquan; Zou, Xiaomao; Hu, Fangzhong; Yao, Changsheng; Liu, Bin; Yang, Huazheng
Journal of Agricultural and Food Chemistry, 2005 , vol. 53, # 24 p. 9566 - 9570
反应条件
1: sodium ethanolate / ethanol / 20 °C 2: ammonium hydroxide / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 11 p. 3579 - 3584
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 112, p. 271
反应条件
diethyl ether Behandeln des nach der Hydrolyse (mit Hilfe von wss. Salzsaeure) erhaltenen Reaktionsprodukts mit wss. Ammoniak unter Zusatz von Ammoniumchlorid;
参考文献
Acta Phytochimica, , vol. 8, p. 65,81
反应条件
Pd-BaSO4; acetic acid Hydrogenation.Erhitzen des Reaktionsprodukts mit wss. Bariumhydroxid;
参考文献
DE545853 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2867
反应条件
Pd-BaSO4; acetic acid T=100°C; Hydrogenation;
参考文献
Frisch; Waldmann
Patent: DE545853 , 1930 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2867