1-(1,3-苯并二氧戊环-5-基)丙-2-烯-1-酮合成路线 （共 7 条）
反应条件
manganese(IV) oxide in dichloromethane T=0°C; 0.5 h;
参考文献
Han, Xiaojun; Corey
Organic Letters, 1999 , vol. 1, # 11 p. 1871 - 1872
反应条件
[Ru(2,2':6':2''-terpyridine)(2,2'-bipyridine)O](2+) in water; tert-butyl alcohol Ambient temperatureelectrolysis in phosphate buffer (pH 6.8);
参考文献
Madurro, Joao Marcos; Chiericato, Glaico Jr.; Giovani, Wagner F.De; Romero, Jose Ricardo
Tetrahedron Letters, 1988 , vol. 29, # 7 p. 765 - 768
反应条件
tin(IV) chloride in dichloromethane T=10 - 15°C; 0.25 h;
参考文献
Daukshas, V. K.; Gaidyalis, P. G.; Udrenaite, E. B.; Labanauskas, L. K.; Gasperavichene, G. A.; et al.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 12 p. 990 - 995
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 12 p. 1466 - 1470
反应条件
1: 97 percent / tetrahydrofuran / 0.5 h / -78 °C 2: 75 percent / MnO2 / CH2Cl2 / 0.5 h / 0 °C View Scheme
参考文献
Han, Xiaojun; Corey
Organic Letters, 1999 , vol. 1, # 11 p. 1871 - 1872
反应条件
18-crown-6 ether; potassium carbonate in benzene 2 h; Reflux;
参考文献
Riofski, Mark V.; John, Jinu P.; Zheng, Mary M.; Kirshner, Julia; Colby, David A.
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 3676 - 3683
反应条件
tin(IV) chloride in dichloromethane T=10 - 15°C; 0.25 h;
参考文献
Daukshas, V. K.; Gaidyalis, P. G.; Udrenaite, E. B.; Labanauskas, L. K.; Gasperavichene, G. A.; et al.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 12 p. 990 - 995
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 12 p. 1466 - 1470
反应条件
1: 78.3 percent / Mg / diethyl ether / 0.75 h / 0 °C 2: 1.) (CH3)2SO4, 2.) 10percent K2CO3 / 1.) ethyl acetate, reflux, 2 h, 2.) benzene, r.t., overnight View Scheme
参考文献
Hayakawa, Satoshi; Michiue, Tohru; Okamoto, Masao; Hatakeyama, Shoko; Ohta, Shunsaku
Heterocycles, 1988 , vol. 27, # 2 p. 457 - 474
