2,7-二(乙酰氨基)芴合成路线 （共 21 条）
反应条件
aluminium trichloride in benzene T=50°C; 0.5 h;
参考文献
Kajigaeshi, Shoji; Kadowaki, Toshiya; Nishida, Akiko; Fujisaki, Shizuo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 97 - 104
反应条件
1: 54 percent / periodic acid, 98percent H2SO4 / H2O 2: 95 percent / copper / 4 h / 230 °C 3: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C 4: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 5: 93 percent / benzene / 0.33 h / 40 - 50 °C 6: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C 2: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 3: 93 percent / benzene / 0.33 h / 40 - 50 °C 4: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: 93 percent / sodium borohydride / ethanol / 0.5 h / Heating 2: 90 percent / hydroiodic acid / acetic acid / 2 h / Heating 3: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C 4: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 5: 93 percent / benzene / 0.33 h / 40 - 50 °C 6: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: 90 percent / hydroiodic acid / acetic acid / 2 h / Heating 2: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C 3: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 4: 93 percent / benzene / 0.33 h / 40 - 50 °C 5: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: 95 percent / copper / 4 h / 230 °C 2: 45 percent / nitric acid, concd. sulfuric acid / acetic anhydride / 2 h / 15 - 20 °C 3: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 4: 93 percent / benzene / 0.33 h / 40 - 50 °C 5: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: 93 percent / benzene / 0.33 h / 40 - 50 °C 2: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: 98 percent / CaCl2, zinc / ethanol; H2O / 2 h / Heating 2: 93 percent / benzene / 0.33 h / 40 - 50 °C 3: 56 percent / AlCl3 / benzene / 0.5 h / 50 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 97 - 104
反应条件
1: glacial acetic acid; fuming nitric acid / 20 °C / man trennt die beiden Isomeren durch fraktionierte Krystallisation aus Eisessig 2: Na2S2O4; diluted alcohol View Scheme
参考文献
Journal of the Chemical Society, , p. 2694
反应条件
1: glacial acetic acid; fuming nitric acid / 20 °C / man trennt die beiden Isomeren durch fraktionierte Krystallisation aus Eisessig 2: Na2S2O4; diluted alcohol View Scheme
参考文献
Journal of the Chemical Society, , p. 2694
