N,N'-(丁二酰二氧基)二琥珀酰亚胺合成路线 (共 3 条)
反应条件
dicyclohexyl-carbodiimide in tetrahydrofuran T=0 - 20°C;
参考文献
ARDELYX, INC.; CHARMOT, Dominique; JACOBS, Jeffrey, W.; LEADBETTER, Michael, Robert; NAVRE, Marc; CARRERAS, Chris; BELL, Noah
Patent: WO2010/78449 A2, 2010 ;
Location in patent: Page/Page column 291 ;
WO 2010/078449 A2
反应条件
triethylamine in acetonitrile 3 h;
参考文献
Hocquelet, Celine; Jankowski, Christopher K.; Pelletier, Andre Lucien; Tabet, Jean-Claude; Lamouroux, Christine; Berthault, Patrick
Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2011 , vol. 69, # 1-2 p. 75 - 84
反应条件
triethylamine in dichloromethane 48 h; other bases, other solvents; Product distribution;
参考文献
Andreev, S. M.; Pavlova, L. A.; Davidovich, Yu. A.; Rogozhin, S. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 5 p. 785 - 789
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 5 p. 1078 - 1081