1-甲氧基-1,3-丁二烯合成路线 (共 11 条)
反应条件
hydrogen; silica gel; BaO T=250°C; P=3800 Torr;
参考文献
Flaig
Chem.Abstr., 1947 , p. 6190
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Flaig
Reichsamt Wirtschaftsausbau Chem.Ber.Pruef.-Nr.093 (P.B. 52020),1073
反应条件
sodium dihydrogenphosphate T=350°C; P=18 Torr;
参考文献
Flaig
Reichsamt Wirtschaftsausbau Chem.Ber.Pruef.-Nr.093Chem.Abstr., (PB 52020)1073 1947 , p. 6190
反应条件
n-butyllithium; potassium tert-butylate; diisopropylamine
参考文献
Margot, Christian; Schlosser, Manfred
Tetrahedron Letters, 1985 , vol. 26, # 8 p. 1035 - 1038
参考文献
Treibs
Angewandte Chemie, 1948 , vol. 60, p. 291
反应条件
hydrogenchloride T=65 - 70°C; 40 h;
参考文献
Khusid, A. Kh.; Yanovskaya, L. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 9 p. 1754 - 1756
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , vol. 30, # 9 p. 2135 - 2137
参考文献
Flaig
Reichsamt Wirtschaftsausbau Chem.Ber.Pruef.-Nr.093(PB 52020)Chem.Abstr., 1073 1947 , p. 6190
参考文献
Treibs
Angewandte Chemie, vol. 60, p. 294
反应条件
Erhitzen des Reaktionsprodukts;
参考文献
Avram; Nenitzescu; Marica
Chemische Berichte, 1957 , vol. 90, p. 1857,1865, 1868
反应条件
sulfuric acid 1.) 3 d; Yield given. Multistep reaction;
参考文献
Bridson, John N.; Bennett, Sharon M.; Butler, Gary
Journal of the Chemical Society, Chemical Communications, 1980 , # 9 p. 413 - 414
反应条件
N-phenyl-N-β-naphthylamine in N,N-dimethyl-formamide T=40°C; Kinetics; regiospecific reaction;
参考文献
Helvetica Chimica Acta, , vol. 91, # 5 p. 783 - 804