4-溴-4'-羟基偶氮苯合成路线 （共 12 条）
参考文献
Shimao, Ichiro; Fujimori, Ken; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 546 - 550
反应条件
sulfuric acid T=50°C; 0.5 h;
参考文献
Shimao, Ichiro; Fujimori, Ken; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 546 - 550
反应条件
in methanol; sulfuric acid; water T=80°C; 0.666667 h;
参考文献
Yamamoto, Jiro; Aimi, Hironori; Masuda, Yasuko; Sumida, Takashi; Umezo, Masahiro; Matuura, Teruo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1565 - 1568
反应条件
1: 4-bromo-aniline With hydrogenchloride; sodium nitrite in water T=0 - 5°C; 2: 4-amino-phenol With sodium hydroxide T=0 - 5°C;
参考文献
Gavin, Jason; Ruiz, Juan F. Marquez; Kedziora, Kinga; Windle, Henry; Kelleher, Dermot P.; Gilmer, John F.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 24 p. 7647 - 7652
反应条件
sulfuric acid T=50°C; 0.5 h;
参考文献
Shimao, Ichiro; Fujimori, Ken; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 546 - 550
反应条件
sulfuric acid T=50°C; 0.5 h;
参考文献
Shimao, Ichiro; Fujimori, Ken; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 546 - 550
反应条件
in methanol; sulfuric acid; water T=70°C; 0.5 h;
参考文献
Yamamoto, Jiro; Aimi, Hironori; Masuda, Yasuko; Sumida, Takashi; Umezo, Masahiro; Matuura, Teruo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1565 - 1568
反应条件
1: 1.) H2O2, 2.) 92percent H2SO4 / 2.) 50 deg C, 30 min 2: 1.) H2O2, 2.) 92percent H2SO4 / 2.) 50 deg C, 30 min View Scheme
参考文献
Shimao, Ichiro; Fujimori, Ken; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 546 - 550
反应条件
hydrogenchloride; sodium nitrite 1.) H2O; Multistep reaction;
参考文献
Guenther, R.; Jaehne, E.; Hartmann, H.; Schulze, M.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 945 - 954
反应条件
sulfuric acid; dihydrogen peroxide 2.) 50 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shimao, Ichiro; Fujimori, Ken; Oae, Shigeru
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 2 p. 546 - 550
