copper(l) iodide in diethyl ether 1.) -78 deg C, 2.) to 10 deg C, 2.5 h;

1: 87 percent / diethyl ether / 21 h / 24 °C 2: 81 percent / 0.5 h / 150 °C 3: 5 percent / H2 / Raney Ni / ethanol / 3 h / 24 °C / other catalysts, solvents, and times View Scheme

Glycine max p83 reductase; NADPH in phosphate buffer T=36°C; pH=7.0; 5 h; Title compound not separated from byproducts;