1,2-二棕榈酰-sn-丙三醇合成路线 （共 18 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethanol; dichloromethane T=20°C; 4 h;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE -CNRS-; UNIVERSITE D'ORLEANS
Patent: US2011/224162 A1, 2011 ;
Location in patent: Page/Page column 10 ;
反应条件
hydrogen; palladium on activated charcoal in ethanol; acetic acid 3 h;
参考文献
Gu, Qu-Ming; Prestwich, Glenn D.
Journal of Organic Chemistry, 1996 , vol. 61, # 24 p. 8642 - 8647
反应条件
hydrogenchloride in methanol; chloroform T=0°C; Substitution; 18 h;
参考文献
Roodsari, Farzaneh S.; Wu, Dongpei; Pum, Gregory S.; Hajdu, Joseph
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7727 - 7737
反应条件
1: With [bis(methyldiphenylphosphine)(1,5-cyclooctadiene)]iridium (1) hexafluorophosphate in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: With iodine in tetrahydrofuran; water T=0°C; 1 h; Inert atmosphere;
参考文献
Fujimoto, Yukari; Mitsunobe, Kunihiro; Fujiwara, Satoko; Mori, Motoko; Hashimoto, Masahiro; Suda, Yasuo; Kusumoto, Shoichi; Fukase, Koichi
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 30 p. 5034 - 5041
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water 0.166667 h; Ambient temperature;
参考文献
Alcaraz, Marie-Lyne; Peng, Ling; Klotz, Philippe; Goeldner, Maurice
Journal of Organic Chemistry, 1996 , vol. 61, # 1 p. 192 - 201
反应条件
1: 96 percent / 4-dimethylaminopyridine; dicyclohexylcarbodiimide / CH2Cl2 / 0 - 20 °C 2: 93 percent / hydrogen; acetic acid / palladium on carbon / ethanol / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 15, # 18 p. 2889 - 2892
反应条件
hydrogenchloride in methanol; chloroform 2 h;
参考文献
Rosseto, Renato; Bibak, Niloufar; Hajdu, Joseph
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 12 p. 2358 - 2360
反应条件
pyridine; triethylamine 2 h; Ambient temperature;
参考文献
Nyilas, Agnes
Nucleosides and Nucleotides, 1998 , vol. 17, # 9-11 p. 1953 - 1967
反应条件
1: 84 percent / pyridine / benzene / 24 h / 60 - 70 °C 2: 97 percent / hydrogen / 10percent Pd/C / hexane / 24 h / 1034.3 - 2585.7 Torr View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 31, # 9 p. 1793 - 1798
反应条件
1: 69.5 percent / DMAP; DCC / CH2Cl2 / 24 h / 20 °C 2: 69.5 percent / BCl3 / CH2Cl2 / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 47, # 11 p. 1659 - 1663
