8-甲氧基-2-甲基喹啉合成路线 （共 34 条）
反应条件
1: 2-methyl-8-hydroxyquinoline With potassium tert-butylate in tetrahydrofuran 3 h; RefluxInert atmosphere; 2: methyl iodide in tetrahydrofuran T=20°C; 6 h; Inert atmosphere;
参考文献
Malecki, Grzegorz; Nycz, Jacek E.; Ryrych, Ewa; Ponikiewski, Lukasz; Nowak, Maria; Kusz, Joachim; Pikies, Jerzy
Journal of Molecular Structure, 2010 , vol. 969, # 1-3 p. 130 - 138
反应条件
12-molybdophosphoric acid HPMo; sodium lauryl sulfate in water; toluene T=80°C; 0.833333 h;
参考文献
Chaskar, Atul; Padalkar, Vikas; Phatangare, Kiran; Langi, Bhushan; Shah, Chetan
Synthetic Communications, 2010 , vol. 40, # 15 p. 2336 - 2340
反应条件
chloranil; trifluoroacetic anhydride in dichloromethane T=20°C; 22 h;
参考文献
Synthesis, , # 15 p. 2415 - 2426
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Chan, Sau Hing; Chui, Chung Hin; Chan, Shun Wan; Kok, Stanton Hon Lun; Chan, Dessy; Tsoi, Miriam Yuen Tung; Leung, Polly Hang Mei; Lam, Alfred King Yin; Chan, Albert Sun Chi; Lam, Kim Hung; Tang, Johnny Cheuk On
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 2 p. 170 - 174
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in dimethyl sulfoxide T=90°C; 17 h;
参考文献
Igarashi, Takeyuki; Inada, Takashi; Sekioka, Tadao; Nakajima, Takayuki; Shimizu, Isao
Chemistry Letters, 2005 , vol. 34, # 1 p. 106 - 107
反应条件
phospho-tungstic acid; phosphotungstic acid; silica gel Doebner-Miller reaction; 0.2 h; microwave irradiation;
参考文献
Sivaprasad, Ganesabaskaran; Rajesh, Rengasamy; Perumal, Paramasivan T.
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1783 - 1785
反应条件
trifluorormethanesulfonic acid; 5A molecular sieve; chloranil; [NBu4][ReO4] in dichloromethane 2 h; Heating;
参考文献
Chemistry Letters, , # 1 p. 5 - 6
反应条件
1: cerium ammonium nitrate / acetonitrile / 0.75 h / 20 °C 2: 85 percent / palladium on activated carbon / toluene / 5 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 3 p. 673 - 681
反应条件
1: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h 2: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h 3: 5 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 22 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2415 - 2426
反应条件
1: 82 percent / aq. NaOH / 1 h 2: 73 percent / H2; HOAc / Pd/C / ethanol / 24 h 3: 44 percent / NH2OH*HCl; pyridine / ethanol / 24 h 4: 5 percent / (CF3CO)2O; 4-chloranil / CH2Cl2 / 22 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2415 - 2426
