dihydrogen peroxide in acetic acid T=80°C; 16 h;

1: 95 percent / SOCl2 / Heating 2: 92 percent / diethyl ether / 2 h / Heating 3: 82 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature 4: 45 percent / 30percent H2O2 / acetic acid / 16 h / 80 °C View Scheme

1: 92 percent / diethyl ether / 2 h / Heating 2: 82 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature 3: 45 percent / 30percent H2O2 / acetic acid / 16 h / 80 °C View Scheme

1: 82 percent / LiAlH4 / diethyl ether / 48 h / Ambient temperature 2: 45 percent / 30percent H2O2 / acetic acid / 16 h / 80 °C View Scheme