(+/-)-1-(9-芴)乙醇合成路线 (共 18 条)
反应条件
sodium tetrahydroborate in methanol T=0 - 5°C; 3 h; Inert atmosphere;
参考文献
Borowiecki, Pawel; Balter, Sylwia; Justyniak, Iwona; Ochal, Zbigniew
Tetrahedron Asymmetry, 2013 , vol. 24, # 18 p. 1120 - 1126
反应条件
pyridine; N-benzyl-trimethylammonium hydroxide T=-10°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 709 - 717
参考文献
Chemische Berichte, , vol. 46, p. 2585
反应条件
1: potassium tert-butylate; sodium t-butanolate / diethyl ether / 3 h / |Reflux 2: sodium tetrahydroborate / methanol / 3 h / 0 - 5 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 24, # 18 p. 1120 - 1126
反应条件
water T=70°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 117, # 37 p. 9399 - 9407
反应条件
sodium isothiocyanate T=70°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 117, # 37 p. 9399 - 9407
反应条件
water T=70°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 117, # 37 p. 9399 - 9407
反应条件
n-butyllithium 1) THF, 2) THF, r.t., 5 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 24 p. 6846 - 6849
参考文献
Annales de Chimie (Cachan, France), , vol. <9> 4, p. 205
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1573 - 1580