3,6-双(氯甲基)杜烯合成路线 （共 12 条）
反应条件
1: acetic acid
2: ethanolic KOH
3: nitrobenzene; NaOH; xylene
View Scheme
参考文献
Esso Research and Eng. Co.
Patent: US2806883 , 1954 ;
反应条件
1: 1.) thiourea, 2.) KOH / 1.) ethanol, 1.5 h, reflux, 2.) H2O, 2 h, reflux
2: 50 percent / 85percent KOH / H2O; methanol; benzene / 72 h
3: 80 percent / various solvent(s) / 4 h / Irradiation
View Scheme
参考文献
Rohrbach, William D.; Boekelheide, V.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3673 - 3678
