3,6-双(氯甲基)杜烯合成路线 （共 12 条）
反应条件
1: With hydrogenchloride; sodium chloride in water T=120°C; 5 h; 2: With zinc(II) chloride in water 24 h; Reflux;
参考文献
Hijazi, Akram; Kemmegne-Mbouguen, Justin Claude; Floquet, Sebastien; Marrot, Jerome; Fize, Jennifer; Artero, Vincent; David, Olivier; Magnier, Emmanuel; Pegot, Bruce; Cadot, Emmanuel
Dalton Transactions, 2013 , vol. 42, # 14 p. 4848 - 4858
反应条件
hydrogenchloride in water T=90°C; Alkylation; 12 h;
参考文献
Olah, George A.; Shamma, Tatyana; Burrichter, Arwed; Rasul, Golam; Prakash, G. K. Surya
Journal of the American Chemical Society, 1997 , vol. 119, # 52 p. 12923 - 12928
反应条件
hydrogenchloride; formaldehyd; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 72, p. 2216,2219
Journal of the Chemical Society, , p. 331,334
反应条件
acetic anhydride; zinc(II) chloride
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, , vol. 21, # 8 p. 1762 - 1772
反应条件
1: acetic acid; potassium acetate / 24 h / 120 °C 2: potassium hydroxide / ethanol / 24 h / 90 °C 3: chromium(VI) oxide; sulfuric acid / water; acetone / 0 - 20 °C View Scheme
参考文献
Hijazi, Akram; Kemmegne-Mbouguen, Justin Claude; Floquet, Sebastien; Marrot, Jerome; Fize, Jennifer; Artero, Vincent; David, Olivier; Magnier, Emmanuel; Pegot, Bruce; Cadot, Emmanuel
Dalton Transactions, 2013 , vol. 42, # 14 p. 4848 - 4858
反应条件
1: acetic acid 2: ethanolic KOH View Scheme
参考文献
Hijazi, Akram; Kemmegne-Mbouguen, Justin Claude; Floquet, Sebastien; Marrot, Jerome; Fize, Jennifer; Artero, Vincent; David, Olivier; Magnier, Emmanuel; Pegot, Bruce; Cadot, Emmanuel
Dalton Transactions, 2013 , vol. 42, # 14 p. 4848 - 4858
反应条件
in diethyl ether; benzene Heating;
参考文献
Reuvers,A.J.M. et al.
Tetrahedron, 1971 , vol. 27, p. 3713 - 3721
反应条件
in acetone 15 h; Heating; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, , vol. 21, # 8 p. 1762 - 1772
反应条件
in N,N-dimethyl-formamide
参考文献
Suzuki,H. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, # 3 p. 836 - 840
