1-溴-4-[(4-氯苯基)甲基]苯合成路线 (共 10 条)
反应条件
trifuran-2-yl-phosphane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
T=25°C;
参考文献
Rottlaender, Mario; Knochel, Paul
Tetrahedron Letters, 1997 , vol. 38, # 10 p. 1749 - 1752
反应条件
potassium hydroxide in diethylene glycol
参考文献
Galun,A.B. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1426 - 1430
反应条件
1: H2SO4
2: KOH / bis-(2-hydroxy-ethyl) ether
View Scheme
参考文献
Galun,A.B. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1426 - 1430
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
参考文献
Blackwell,J.; Hickinbottom,W.J.
Journal of the Chemical Society, 1961 , p. 1405 - 1407
反应条件
boron trifluoride diethyl etherate
T=25°C; Friedel Crafts alkylation; 24 h; Inert atmosphere;
参考文献
Schaefer, Gabriel; Bode, Jeffrey W.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 46 p. 10913 - 10916
反应条件
silica gel supported phosphorus pentoxide
T=20°C; 0.166667 h; Neat (no solvent);
参考文献
Khazaei, Ardeshir; Rad, Mohammad Navid Soltani; Borazjani, Maryam Kiani; Moradian, Khadijeh Mansouri; Borazjani, Mohammad Kiani; Zebarjadian, Mohammad Hassan
South African Journal of Chemistry, 2011 , vol. 64, p. 120 - 126
反应条件
in chlorobenzene
T=120°C; 4 h;
参考文献
Katritzky, Alan R.; Marson, Charles M.; Chen, Jen-Luan; Saczewski, Franciszek; King, Roy W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1331 - 1336
参考文献
Katritzky, Alan R.; Marson, Charles M.; Chen, Jen-Luan; Saczewski, Franciszek; King, Roy W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1331 - 1336
参考文献
Blackwell,J.; Hickinbottom,W.J.
Journal of the Chemical Society, 1963 , p. 366 - 373
反应条件
Pd(dippp)2 in benzene
T=90°C; Methylation; 22 h;
参考文献
Blum, Jochanan; Berlin, Olga; Milstein, David; Ben-David, Yehoshua; Wassermann, Birgit C.; Schutte, Stefan; Schumann, Herbert
Synthesis, 2000 , # 4 p. 571 - 575