in water-d2
D2O added dropwise to a mixt. of NaCN and P2O5 under N2; collected in cooled trip; purified by pumping on the cooled in a CO2/acetone slush bath;
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Chemical Physics, 2005 , vol. 309, # 2-3 p. 291 - 301
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Anderson, J. R.; Clark, N. J.
C.A., Proc. 3-rd Intern. Congr. Catalysis, Amsterdam 1964 (1965),, Bd. 2, S. 1048/62 1965 , vol. 63, p. 12665
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Gmelin Handbook: C: MVol.D1, 15.4.2.3, page 127 - 161
Kinetics; byproducts: D, D2; in mass spectrometer at 1 Torr total pressure and various temperatures with a linear flow velocity between 1500-3200 cm/s (depending on temperature); product ratio independent of T from 200K-363K;; products not isolated; detected by mass spectroscopy;
参考文献
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