in diethyl ether at -75°C, pptn.;; washing with acetonitrile, drying at 70°C and 0.1Torr;;
参考文献
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
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Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
in diethyl ether at -75°C, pptn.;; washing with acetonitrile, drying at 70°C and 0.1Torr;;
参考文献
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
Full Text View citing articles Show Details
Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
Full Text View citing articles Show Details
Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
in further solvent(s) byproducts: Me3SiF, C6H5F; AgF suspended in EtCN at room temp., Si compd. added, stirred for 30-60 min; volatiles distd. in vac., at elevated temp. (40°C), elem. anal.;
参考文献
Tyrra, Wieland; Wickleder, Mathias S.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 8 p. 1841 - 1847
Smith, V. B.; Massey, A. G.
Journal of Organometallic Chemistry, 1970 , vol. 23, p. C9 - C10
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Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
in further solvent(s) byproducts: Ag; To soln. of Ag compd. in EtCN or PrCN twofold or stoich. amt. of elementadded, warmed at 65°C for 16 h; extd. with n-pentane, eluent evapd. in vac. at 0°C, purity checked by elem. anal., mass, (19)F and (13)C NMR spectra;
参考文献
Tyrra, Wieland; Wickleder, Mathias S.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2002 , vol. 628, # 8 p. 1841 - 1847
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
Full Text View citing articles Show Details
Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
Full Text View citing articles Show Details
Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
Miller, W. T.; Sun, K. K.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6985 - 6987
Full Text View citing articles Show Details
Gmelin Handbook: Ag: MVol.B5, 1.1.3, page 8 - 12
