反应条件
in benzene a soln. in benzene of ligand and Pb-acetate was kept at room temp. for 3 h, pptn. of Pb(CH3COO)2; filtn., filtrate volume was reduced by boiling, addn. of boiling MeOH, standing, sepn. of product, flash chromy. (Kieselgel, CHCl3 as eluant), concn. of major band, addn. of MeOH, ppt. was washed (MeOH), dried in vacuo at 80°C, elem. anal.;
参考文献
Inorganic Chemistry, , vol. 30, p. 4160 - 4165
