(2-硝基苯基)乙酸甲酯合成路线 (共 35 条)
参考文献
Journal of the American Chemical Society, , vol. 59, p. 2348,2350
反应条件
Ph3PCH2PhNO3; trifluoromethanesulfonic anhydride T=20°C; 0.333333 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 179, # 2 p. 221 - 226
反应条件
iodine in dimethyl sulfoxide Acidic conditions;
参考文献
Synthetic Communications, , vol. 43, # 14 p. 1955 - 1963
参考文献
Singh, Jujhar; Nigam, M. B.; Sardana, Vinod; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 596 - 597
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 2 p. 548 - 551
反应条件
T=60°C; Product distribution;
参考文献
Singh, Jujhar; Nigam, M. B.; Sardana, Vinod; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 596 - 597
反应条件
1: 97 percent / H2 / 5percent Pd/C / toluene / Ambient temperature 2: 71 percent / 90percent t-BuONO / toluene / 1.5 h / 90 - 95 °C View Scheme
参考文献
Heterocycles, , vol. 43, # 12 p. 2701 - 2712
反应条件
hydrogen; 10 percent Pd/C contd. 50percent water in ethyl acetate T=20°C; atmospheric pressure;
参考文献
Katayama, Seiji; Ae, Nobuyuki; Kodo, Toru; Masumoto, Shuji; Hourai, Shinji; Tamamura, Chika; Tanaka, Hiroyasu; Nagata, Ryu
Journal of Medicinal Chemistry, 2003 , vol. 46, # 5 p. 691 - 701
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate T=0°C; P=735.5 Torr; 4 h; Title compound not separated from byproducts;
参考文献
Motoyama, Yukihiro; Kamo, Kazuyuki; Nagashima, Hideo
Organic Letters, 2009 , vol. 11, # 6 p. 1345 - 1348
反应条件
1: 97 percent / H2 / 5percent Pd/C / toluene / Ambient temperature 2: 87 percent / 90percent t-BuONO / acetic acid / 0.5 h / 90 - 95 °C 3: 97 percent / NaOH, water / 1.5 h / Heating View Scheme
参考文献
Yoshida, Toyokichi; Matsuura, Noriyasu; Yamamoto, Katsuhisa; Doi, Masahiro; Shimada, Kanji; Morie, Toshiya; Kato, Shiro
Heterocycles, 1996 , vol. 43, # 12 p. 2701 - 2712