(2S,3R,4E)-3-苯甲酰基-2-叔-丁基氧羰基氨基-4-十八碳烯-1,3-二醇合成路线 (共 3 条)
反应条件
Multi-step reaction with 3 steps 1: 35 percent / Red-Al / toluene; diethyl ether / 22 h / 20 °C2: 53 percent / pyridine; DMAP / 2 h3: 43 percent / trifluoroacetic acid / 3 h
参考文献
Duffin, Gordon R.; Ellames, George J.; Hartmann, Sascha; Herbert, John M.; Smith, David I. Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 14 p. 2237 - 2242
反应条件
Multi-step reaction with 2 steps 1: 72 percent / diisopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 36 h2: 43 percent / trifluoroacetic acid / 3 h
参考文献
Duffin, Gordon R.; Ellames, George J.; Hartmann, Sascha; Herbert, John M.; Smith, David I. Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 14 p. 2237 - 2242
反应条件
Multi-step reaction with 2 steps 1: 53 percent / pyridine; DMAP / 2 h2: 43 percent / trifluoroacetic acid / 3 h
参考文献
Duffin, Gordon R.; Ellames, George J.; Hartmann, Sascha; Herbert, John M.; Smith, David I. Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 14 p. 2237 - 2242