2,3,4-戊三酮肟 (6ci,7ci,8ci,9ci)合成路线 （共 37 条）
反应条件
potassium tert-butylate in tert-butyl alcohol var. reagents, var. solvents; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1299 - 1304
Zhurnal Organicheskoi Khimii, , vol. 18, # 7 p. 1489 - 1495
反应条件
1: water; hydroxylamine hydrochloride 2: ueber den Schmelzpunkt View Scheme
参考文献
Ponzio; Ruggeri
Gazzetta Chimica Italiana, 1922 , vol. 52 I, p. 296
Gazzetta Chimica Italiana, 1923 , vol. 53, p. 300
反应条件
hydroxylamine hydrochloride; sodium acetate in water T=80°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Fruttero, Roberta; Calvino, Rosella; Ferrarotti, Bruno; Gasco, Alberto; Aime, Silvio; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 523 - 530
反应条件
acetic acid
T=100°C; 4 h;
参考文献
Budyka, M. F.; Kantor, M. M.; Alfimov, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 10 p. 1072 - 1075
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 10 p. 1340 - 1343
反应条件
1: benzene
2: aqueous H2SO4; FeCl3
View Scheme
参考文献
Barltrop et al.
Journal of the Chemical Society, 1959 , p. 1132,1133
反应条件
1: HCl / acetic acid / 2 h / 0 - 5 °C
2: 0.531 g / zinc; AcOH / 0.5 h / 40 °C
View Scheme
参考文献
Cai, Xiao-hua; Yang, Hai-jun; Zhang, Guo-lin
Synthesis, 2005 , # 10 p. 1569 - 1571
参考文献
Cuadrado, Purificacion; Gonzalez-Nogal, Ana M.; Martinez, Senen
Tetrahedron, 1997 , vol. 53, # 25 p. 8585 - 8598
参考文献
Cameron, Mailer; Gowenlock, Brian G.; Boyd, Alan S. F.
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 0, # 11 art. no. 6/03713E, p. 2271 - 2274
参考文献
Wolff
Justus Liebigs Annalen der Chemie, 1902 , vol. 325, p. 137
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 46 Anm. 2
参考文献
Wolff
Justus Liebigs Annalen der Chemie, vol. 325, p. 192
