氯(二甲基硫化)金(I)合成路线 (共 39 条)
反应条件
in dichloromethane; acetone byproducts: Cl(1-); addn. of (AuCl(SMe2)) in CH2Cl2 to a soln. of Pt-compd. in acetone, stirred for 1 h; volume reduced, addn. of pentane; elem. anal.;
参考文献
Hadj-Bagheri, Nasim; Puddephatt, Richard J.
Inorganica Chimica Acta, 1993 , vol. 213, p. 29 - 40
反应条件
in dichloromethane refluxed for 2 h; evapd. to dryness, stirred under Et2O for 24 h, filtered, washed with Et2O; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in dichloromethane refluxed for 2 h; concd. under reduced pressure, filtered, washed with CH2Cl2; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in dichloromethane refluxed for 2 h; concd. under reduced pressure, filtered, washed with CH2Cl2; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in dichloromethane refluxed for 2 h; concd. under reduced pressure, filtered, washed with CH2Cl2; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in dichloromethane refluxed for 2 h; concd. under reduced pressure, addn. of Et2O, filtered, treated with hot petroleum ether; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in dichloromethane refluxed for 2 h; concd. under reduced pressure, filtered, washed with CH2Cl2; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in dichloromethane-d2 To a soln. of Pt(CH3)2(C5H4N)2 is added a soln. of AuCl(S(CH3)2) at -70°C, warming up to -10°C.; Monitored by NMR.;
参考文献
Arsenault, Gilles J.; Anderson, Craig M.; Puddephatt, Richard J.
Organometallics, 1988 , vol. 7, p. 2094 - 2097
反应条件
in dichloromethane refluxed for 2 h; concd. under reduced pressure, filtered, washed with CH2Cl2; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488
反应条件
in methanol refluxed for 2 h; concd. under reduced pressure, filtered, washed with CH2Cl2; elem. anal.;
参考文献
Leonesi, Dante; Lorenzotti, Adriana; Cingolani, Augusto; Bonati, Flavio
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 483 - 488