1-(4-甲氧基苯基)-2-硝基丙烷合成路线 （共 8 条）
反应条件
hydrogenchloride; iron in methanol; water 0.5 h; Heating;
参考文献
Pradhan, Prasun K.; Dey, Sumit; Jaisankar, Parasuraman; Giri, Venkatachalam S.
Synthetic Communications, 2005 , vol. 35, # 7 p. 913 - 922
反应条件
acetic acid; sodium nitrite in dimethyl sulfoxide T=35°C; 1.5 h;
参考文献
Ran, Chongzhao; Yang, Genjin; Wu, Taizhi; Xie, Meihua
Tetrahedron Letters, 2003 , vol. 44, # 44 p. 8061 - 8062
反应条件
formic acid; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; triethylamine; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide in ethyl acetate
T=28°C; 5 h; chemoselective reaction;
参考文献
Xiang, Jing; Sun, Er-Xiao; Lian, Chun-Xia; Yuan, Wei-Cheng; Zhu, Jin; Wang, Qiwei; Deng, Jingen
Tetrahedron, 2012 , vol. 68, # 24 p. 4609 - 4620
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; silica gel in benzene
T=60°C; 20 h;
参考文献
FUJI, Masayuki
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 11 p. 4029 - 4036
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene
T=150°C; Wadsworth-Emmons reaction; 72 h;
参考文献
Black, Phillip. J.; Cami-Kobeci, Gerta; Edwards, Michael G.; Slatford, Paul A.; Whittlesey, Michael K.; Williams, Jonathan M. J.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 1 p. 116 - 125
反应条件
1: 48 percent / ammonium acetate / Heating
2: 66 percent / baker's yeast / ethanol; H2O / 24 h / 35 °C
View Scheme
参考文献
Kawai, Yasushi; Inaba, Yoshikazu; Tokitoh, Norihiro
Tetrahedron Asymmetry, 2001 , vol. 12, # 2 p. 309 - 318
反应条件
1: sodium carbonate / benzene / 5 h / Heating
2: 100 percent / 3,5-bis(ethoxycarbonyl)-2,6-dimethyl-1,4-dihydropyridine, silica gel / benzene / 0.5 h / Heating
View Scheme
参考文献
FUJI, Masayuki
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 11 p. 4029 - 4036
反应条件
1: pyridine / 2 h / Ambient temperature
2: sodium carbonate / benzene / 5 h / Heating
3: 100 percent / 3,5-bis(ethoxycarbonyl)-2,6-dimethyl-1,4-dihydropyridine, silica gel / benzene / 0.5 h / Heating
View Scheme
参考文献
FUJI, Masayuki
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 11 p. 4029 - 4036
