2-甲基-2-疏基硫酸脲合成路线 （共 72 条）
参考文献
Bredereck et al.
Angewandte Chemie, 1959 , vol. 71, p. 753,757
Chemische Berichte, 1962 , vol. 95, p. 2049,2052,2053
反应条件
1: With sodium ethanolate in ethanol Heating; 2: With sodium hydroxide in tetrahydrofuran; methanol T=20°C;
参考文献
Palanki, Moorthy S.S.; Gayo-Fung, Leah M.; Shevlin, Graziella I.; Erdman, Paul; Sato, Mark; Goldman, Mark; Ransone, Lynn J.; Spooner, Cheryl
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 18 p. 2573 - 2577
参考文献
Cowie; Gibson
Journal of the Chemical Society, 1934 , p. 46
反应条件
triethylamine in ethanol 48 h; Reflux;
参考文献
MERCK PATENT GMBH; SCHIEMANN, Kai; SCHULTZ, Melanie; STAEHLE, Wolfgang; KOBER, Ingo; WIENKE, Dirk; KRIER, Mireille
Patent: WO2010/63352 A1, 2010 ;
Location in patent: Page/Page column 88-89 ;
WO 2010/063352 A1
参考文献
Yoshikawa
Yakugaku Zasshi, 1956 , vol. 76, p. 776
Chem.Abstr., 1957 , p. 1197
反应条件
in water 6 h; Reflux;
参考文献
Zhang, Fan; Zhai, Xin; Chen, Li Juan; Qi, Jian Guo; Cui, Bo; Gu, Yu Cheng; Gong, Ping
Chinese Chemical Letters, 2011 , vol. 22, # 11 p. 1277 - 1280
参考文献
Todd; Fletcher; Tarbell
Journal of the American Chemical Society, 1943 , vol. 65, p. 350,352
参考文献
Vanderhaeghe
Bulletin des Societes Chimiques Belges, 1953 , vol. 62, p. 611,617
反应条件
methanol; bromine; sodium methylate
参考文献
Goerdeler; Linden
Chemische Berichte, 1956 , vol. 89, p. 2742,2744, 2745
反应条件
unter vermindertem Druck;
参考文献
King
Journal of the Chemical Society, 1930 , p. 2376
