2-乙酰氨基-2-脱氧-beta-d-吡喃葡萄糖叠氮化物合成路线 （共 18 条）
反应条件
sodium in methanol T=20°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 24 p. 7736 - 7745
反应条件
sodium azide; 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine in water T=0°C; 1 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 6 p. 942 - 955
反应条件
sodium azide in N,N-dimethyl-formamide T=20°C;
参考文献
Organic Letters, , vol. 10, # 16 p. 3461 - 3463
反应条件
1: 100 percent / NaN3; TBAHS; aq. NaHCO3 / CH2Cl2 2: NaOMe / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 7 p. 1325 - 1328
反应条件
1.1: 20 °C 2.1: sodium azide / N,N-dimethyl-formamide / 70 °C 3.1: magnesium; methanol / 3 h / 20 °C / |Inert atmosphere 3.2: Amberlyst 15 ion exchange resin / 0.17 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 732 - 735
反应条件
1.1: sodium azide / N,N-dimethyl-formamide / 70 °C 2.1: magnesium; methanol / 3 h / 20 °C / |Inert atmosphere 2.2: Amberlyst 15 ion exchange resin / 0.17 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 732 - 735
反应条件
1.1: sodium methylate / methanol 1.2: 0 - 20 °C 2.1: 20 °C 3.1: sodium azide / N,N-dimethyl-formamide / 70 °C 4.1: magnesium; methanol / 3 h / 20 °C / |Inert atmosphere 4.2: Amberlyst 15 ion exchange resin / 0.17 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 732 - 735
反应条件
1: 79.5 percent / trimethylsilyl azide, SnCl4 / CH2Cl2 / 40 h / Ambient temperature 2: 84.5 percent / 1 M NaOMe / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 143, p. 21 - 42
反应条件
1: 73.4 percent / trimethylsilyl azide, SnCl4 / CH2Cl2 / 24 h 2: 84.5 percent / 1 M NaOMe / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 143, p. 21 - 42
反应条件
1: 74 percent / trimethylsilyl azide, SnCl4 / CH2Cl2 2: 84.5 percent / 1 M NaOMe / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 143, p. 21 - 42
